Effect of thickness of indirect restoration and distance from the light-curing unit tip on the hardness of a dual-cured resin cement

This study evaluated the Knoop hardness and polymerization depth of a dual-cured resin cement, light-activated at different distances through different thicknesses of composite resin. One bovine incisor was embedded in resin and its buccal surface was flattened. Dentin was covered with PVC film where a mold (0.8-mm-thick and 5 mm diameter) was filled with cement and covered with another PVC film. Light curing (40 s) was carried out through resin discs (2, 3, 4 or 5 mm) with a halogen light positioned 0, 1, 2 or 3 mm from the resin surface. After storage, specimens were sectioned for hardness measurements (top, center, and bottom). Data were subjected to split-plot ANOVA and Tukey's test (α=0.05). The increase in resin disc thickness decreased cement hardness. The increase in the distance of the light curing tip decreased hardness at the top region. Specimens showed the lowest hardness values at the bottom, and the highest at the center. Resin cement hardness was influenced by the thickness of the indirect restoration and by the distance between the light-curing unit tip and the resin cement surface.Piracicaba Dental School State University of Campinas, Piracicaba, SPDepartment of Dental Materials and Prosthodontics São José dos Campos Dental School São Paulo State University, São José dos Campos, SPDepartment of Restorative Dentistry Piracicaba Dental School State University of Campinas, Piracicaba, SPDepartment of Pediatric Dentistry Piracicaba Dental School State University of Campinas, Piracicaba, SPDepartment of Dental Materials and Prosthodontics São José dos Campos Dental School São Paulo State University, São José dos Campos, S

Effects of Preheating and Precooling on the Hardness and Shrinkage of a Composite Resin Cured with QTH and LED

SUMMARY The aim of this study was to evaluate in vitro the hardness and shrinkage of a pre-cooled or preheated hybrid composite resin cured by a quartz-tungsten-halogen light (QTH) and light-emitting diode (LED) curing units. The temperature on the tip of the devices was also investigated. Specimens of Charisma resin composite were produced with a metal mold kept under 37°C. The syringes were submitted to 4°C, 23°C, and 60°C (n=20) before light-curing, which was carried out with the Optilux 501 VCL and Elipar FreeLight 2 units for 20 seconds. The specimens were kept under 37°C in a high humidity condition and darkness for 48 hours. The Knoop hardness test was carried out with a 50 gram-force (gf) load for 10 seconds, and the measurement of the shrinkage gap was carried out using an optical microscope. The data were subjected to analysis of variance and the Games-Howell test (α=0.05). The mean hardness of the groups were similar, irrespective of the temperatures (p&amp;gt;0.05). For 4°C and 60°C, the top surface light-cured by LED presented significantly reduced shrinkage when compared with the bottom and to both surfaces cured by QTH (p&amp;lt;0.05). It was concluded that the hardness was not affected by pre-cooling or preheating. However, polymerization shrinkage was slightly affected by different pre-polymerization temperatures. The QTH-curing generated greater shrinkage than LED-curing only when the composite was preheated. Different temperatures did not affect the composite hardness and shrinkage when cured by a LED curing unit.</jats:p

Influence of curing tip distance on resin composite Knoop Hardness Number, using three different light curing units

This in vitro study evaluated the influence of curing tip distance on the Knoop Hardness Number (KHN) of a resin composite when using three different light curing units: (1) a halogen light (XL 1500 curing unit-3M), (2) a "softstart-polymerization" (Elipar Trilight curing in an exponential mode-ESPE) and (3) a PAC (Apolo 95E curing unit-DMD). The resin composite, Filtek Z250 (3M), was cured by these curing units at three. light-tip distances from the resin composite: 0 mm, 6 mm and 12 mm. The resin composite specimens were flattened to their middle portion and submitted to 18 KHN measurements per specimen. The results showed that for the Elipar Trilight unit, the hardness of the resin composite decreased as the light tip distance increased. The XL 1500 unit presented a significant decrease in hardness as the depth of cure of the resin composite increased. Apolo 95E caused a decrease in the resin composite hardness values when the depth of cure and light tip distance increased.28331532

Marginal Adaptation and Quality of Interfaces in Lithium Disilicate Crowns — Influence of Manufacturing and Cementation Techniques

SUMMARY Purpose: To evaluate the cement line thickness and the interface quality in milled or injected lithium disilicate ceramic restorations and their influence on marginal adaptation using different cement types and different adhesive cementation techniques. Methods and Materials: Sixty-four bovine teeth were prepared for full crown restoration (7.0±0.5 mm in height, 8.0 mm in cervical diameter, and 4.2 mm in incisal diameter) and were divided into two groups: CAD/CAM automation technology, IPS e.max CAD (CAD), and isostatic injection by heat technology, IPS e.max Press (PRESS). RelyX ARC (ARC) and RelyX U200 resin cements were used as luting agents in two activation methods: initial self-activation and light pre-activation for one second (tack-cure). Next, the specimens were stored in distilled water at 23°C ± 2°C for 72 hours. The cement line thickness was measured in micrometers, and the interface quality received scores according to the characteristics and sealing aspects. The evaluations were performed with an optical microscope, and scanning electron microscope images were presented to demonstrate the various features found in the cement line. For the cement line thickness, data were analyzed with three-way analysis of variance (ANOVA) and the Games-Howell test (α=0.05). For the variable interface quality, the data were analyzed with the Mann-Whitney U-test, the Kruskal-Wallis test, and multiple comparisons nonparametric Dunn test (α=0.05). Results: The ANOVA presented statistical differences among the ceramic restoration manufacturing methods as well as a significant interaction between the manufacturing methods and types of cement (p&amp;lt;0.05). The U200 presented lower cement line thickness values when compared to the ARC with both cementation techniques (p&amp;lt;0.05). With regard to the interface quality, the Mann-Whitney U-test and the Kruskal-Wallis test demonstrated statistical differences between the ceramic restoration manufacturing methods and cementation techniques. The PRESS ceramics obtained lower scores than did the CAD ceramics when using ARC cement (p&amp;lt;0.05). Conclusions: Milled restorations cemented with self-adhesive resin cement resulted in a thinner cement line that is statistically different from that of CAD or pressed ceramics cemented with resin cement with adhesive application. No difference between one-second tack-cure and self-activation was noted.</jats:p

Effect of light curing tip distance and resin shade on microhardness of a hybrid resin composite Efeito da distância da ponta do aparelho de fotoativação e da cor na microdureza superficial de um compósito híbrido

Resin composite shades and resin composite polymerization performed with a distanced light tip are factors that can affect polymerization effectiveness. Thisin vitro study aimed to evaluate the influence of curing tip distance and resin shade on the microhardness of a hybrid resin composite (Z250 - 3M ESPE). Forty-five resin composite specimens were randomly prepared and divided into nine experimental groups (n = 5): three curing tip distances (2 mm, 4 mm, and 8 mm) and three resin shades (A1, A3.5, and C2). All samples were polymerized with a continuous output at 550 mW/cm². After 24 hours, Knoop microhardness measurements were obtained on the top and bottom surfaces of the sample, with a load of 25 grams for 10 seconds. Five indentations were performed on each surface of each sample. Results showed that bottom surface samples light-cured at 2 mm and 4 mm presented significantly higher hardness values than samples light-cured at 8 mm. The resin shade A1 presented higher hardness values and was statistically different from C2. The resin shade A3.5 did not present statistical differences from A1 and C2. For the top surface, there were no statistical differences among the curing tip distances. For all experimental conditions, the top surface showed higher hardness values than the bottom surface. It was concluded that light curing tip distance and resin shade are important factors to be considered for obtaining adequate polymerization.<br>A cor do compósito e a polimerização realizada com a ponta do aparelho de fotoativação distante da superfície do compósito são fatores que podem afetar a efetividade de polimerização. Assim, o objetivo deste estudo in vitro foi avaliar a influência desses fatores na microdureza superficial de um compósito híbrido (Z250 - 3M ESPE). Quarenta e cinco espécimes de compósito foram aleatoriamente preparados de acordo com os nove grupos experimentais (n = 5): três distâncias de fotoativação (2 mm, 4 mm e 8 mm) e três cores de compósito (A1, A3,5 e C2). Todas as amostras foram fotoativadas com aparelho de fotoativação ajustado com intensidade contínua de 550 mW/cm². Após 24 horas, dez medidas de dureza Knoop foram obtidas nas superfícies de topo e fundo de cada amostra, com carga de 25 gramas por um tempo de 10 segundos. Resultados mostraram que, para a superfície de fundo, os grupos com a fotoativação realizada com distância de 2 e 4 mm apresentaram maiores médias do que os grupos com distância de 8 mm, e os grupos de cor A1 apresentaram maiores médias e com diferenças estatísticas que os grupos de cor C2, e o grupo A3,5 não apresentou diferenças estatísticas quando comparado aos outros grupos. Para a superfície de topo, não houve diferenças estatísticas significantes para os fatores estudados. Para todas as condições experimentais, a superfície de fundo apresentou médias de durezas estatisticamente menores do que as da superfície de topo. Pode-se concluir que os fatores cor do compósito e distância de polimerização são importantes fatores a serem considerados para a obtenção de adequada polimerização

Influence of different light-curing units on the surface roughness of restorative materials: in situ study

The aim of this study was to evaluate the influence of different light sources (LED and Halogen lamp) on the roughness (superficial) of composite resin (Filtek Z250, Filtek P60, Charisma and Durafill) varying post-irradiation times, in an in situ experiment. For this purpose, 80 specimens were made in polyurethane moulds. Ten volunteers without medicament use and good oral condition were selected and from them study moulds were obtained. A palatal intra-oral acrylic resin appliance was made for each of the subjects of the experiment. In each appliance, two specimens of each material were fixed (LED/Halogen lamp - control group). Roughness tests were performed immediately and 30 days after initial light-curing. Statistical analysis was performed using ANOVA. Statistically significant difference was observed only between post-irradiation times, where the 30th day showed the highest roughness values. It be concluded that roughness was influenced only by post-irradiation times, presenting the 30- days period inferior behavior