Mechanical loss in state-of-the-art amorphous optical coatings

We present the results of mechanical characterizations of many different high-quality optical coatings made of ion-beam-sputtered titania-doped tantala and silica, developed originally for interferometric gravitational-wave detectors. Our data show that in multi-layer stacks (like high-reflection Bragg mirrors, for example) the measured coating dissipation is systematically higher than the expectation and is correlated with the stress condition in the sample. This has a particular relevance for the noise budget of current advanced gravitational-wave interferometers, and, more generally, for any experiment involving thermal-noise limited optical cavities.Comment: 31 pages, 14 figure

Material loss angles from direct measurements of broadband thermal noise

International audienceWe estimate the loss angles of the materials currently used in the highly reflective test-mass coatings of interferometric detectors of gravitational waves, namely Silica, Tantala, and Ti-doped Tantala, from direct measurement of coating thermal noise in an optical interferometer testbench, the Caltech TNI. We also present a simple predictive theory for the material properties of amorphous glassy oxide mixtures, which gives results in good agreement with our measurements on Ti-doped Tantala. Alternative measurement methods and results are reviewed, and some critical issues are discussed

Measurements of mechanical thermal noise and energy dissipation in optical dielectric coatings

In recent years an increasing number of devices and experiments are shown to be limited by mechanical thermal noise. In particular sub-Hertz laser frequency stabilization and gravitational wave detectors, that are able to measure fluctuations of 1E-18 m/rtHz or less, are being limited by thermal noise in the dielectric coatings deposited on mirrors. In this paper we present a new measurement of thermal noise in low absorption dielectric coatings deposited on micro-cantilevers and we compare it with the results obtained from the mechanical loss measurements. The coating thermal noise is measured on the widest range of frequencies with the highest signal to noise ratio ever achieved. In addition we present a novel technique to deduce the coating mechanical losses from the measurement of the mechanical quality factor which does not rely on the knowledge of the coating and substrate Young moduli. The dielectric coatings are deposited by ion beam sputtering. The results presented here give a frequency independent loss angle of (4.70 $\pm$ 0.2)x1E-4 with a Young's modulus of 118 GPa for annealed tantala from 10 Hz to 20 kHz. For as-deposited silica, a weak frequency dependence (~ f^{-0.025}) is observed in this frequency range, with a Young's modulus of 70 GPa and an internal damping of (6.0 $\pm$ 0.3)x1E-4 at 16 kHz, but this value decreases by one order of magnitude after annealing and the frequency dependence disappears.Comment: Accepted for publication in Phys. Rev.

Correlated evolution of structure and mechanical loss of a sputtered silica film

Energy dissipation in amorphous coatings severely affects high-precision optical and quantum transducers. In order to isolate the source of coating loss, we performed an extensive study of Raman scattering and mechanical loss of a thermally-treated sputtered silica coating. Our results show that loss is correlated with the population of three-membered rings of Si-O$_4$ tetrahedral units, and support the evidence that thermal treatment reduces the density of metastable states separated by a characteristic energy of about 0.5 eV, in favour of an increase of the states separated by smaller activation energies. Finally, we conclude that three-fold rings are involved in the relaxation mechanisms only if they belong to more complex chain-like structures of 10 to 100 tetrahedra.Comment: 5 pages, 3 figure

A new method of probing mechanical losses of coatings at cryogenic temperatures

A new method of probing mechanical losses and comparing the corresponding deposition processes of metallic and dielectric coatings in 1-100 MHz frequency range and cryogenic temperatures is presented. The method is based on the use of extremely high-quality quartz acoustic cavities whose internal losses are orders of magnitude lower than any available coatings nowadays. The approach is demonstrated for Chromium, Chromium/Gold and a multilayer tantala/silica coatings. The ${\rm Ta}_2{\rm O}_5/{\rm Si}{\rm O}_2$ coating has been found to exhibit a loss angle lower than $1.6\times10^{-5}$ near 30 {\rm MHz} at 4 {\rm K}. The results are compared to the previous measurements

Etude des oxynitrures de silicium en couches minces déposées par pulvérisation en vue d'applications optiques

This work is based n the study of silicon oxynitride thin films, deposited by RF magnetron sputtering, to realize low losses optical multilayers (absorption, sputtering).At first, we have analysed the variations of the optical and physicochemical properties of the oxynitrides monolayers due to the deposition parameters : the gas partial pressures, the RF power, the target composition, the gas mixture. So, by describing the whole oxynitrides domain from the oxyde to the nitride, we have shown the linear variation of the refractive index as well as the strict substitution of oxygen atoms by nitrogen atoms : this is the proof of a simple mechanism of formation. Moreover, thanks to IR spectrophotometric analyses, a model of the oxynitrides amorphous structure has been proposed and confirmed by two approximation methods.At last, we have studied more precisely the absorption (photothermal deflection) and the scattering (scatterrometer CASI) levels of the monolayers and the multilayers synthetized from silicon oxynitrides (antireflective stacks, mirrors). A comparison with the optical performances of classical stacks made of oxide, deposited by ion beam sputtering, have been made and we have proposed some solutions to decrease the two sources of losses.Ce travail repose sur l'étude des couches minces d'oxynitrures de silicium obtenues par pulvérisations radio-fréquence magnétron réactive en vue de réaliser des multicouches optiques de faibles pertes (absorption, diffusion).Tout d'abord, nous avons analysé les variations des propiétés optiques et physicochimiques des couches d'oxynitrures liées aux différents paramètres du bâti de dépôt : les pressionspartielles des gaz, la puissance RF, la nature de la cible et des gaz.Ainsi, lorsque l'on décrit toute la gamme des oxynitrures de l'oxyde au nitrure, nous avons en particulier mis en évidence l'évolution quasi linéaire de l'indice sur un domaine relativement important ainsi que la substitution rigoureuse des atomes d'oxygène par les atomes d'azote : ceci est la preuve d'un mécanisme simple de formation. De plus, grâce à des analyses par spectrophotométrie IR, un modèle de la structure amorphe des oxynitrures a été proposé : (pseudo-binaire oxyde-nitrure) et vérifié par deux méthodes d'approxmation. Enfin, une étude plus particulière de l'absorption (photothermie) et de la diffusion( diffusomètre CASI) a été menée sur les couches et sur les multicouches synthétisés à partir des oxynitrures (Antireflets, Miroirs). Une comparaison avec les performaces des empilements classiques d'oxydes réalisés par pulvérisation par faisceaux d'ions a pu être faite et nous avons ainsi proposé des solutions pour optimiser les deux sources de pertes

Estimation of losses in a 300 m filter cavity and quantum noise reduction in the KAGRA gravitational-wave detector

International audienceThe sensitivity of the gravitational-wave detector KAGRA, presently under construction, will be limited by quantum noise in a large fraction of its spectrum. The most promising technique to increase the detector sensitivity is the injection of squeezed states of light, where the squeezing angle is dynamically rotated by a Fabry-Pérot filter cavity. One of the main issues in the filter cavity design and realization is the optical losses due to the mirror surface imperfections. In this work we present a study of the specifications for the mirrors to be used in a 300 m filter cavity for the KAGRA detector. A prototype of the cavity will be constructed at the National Astronomical Observatory of Japan, inside the infrastructure of the former TAMA interferometer. We also discuss the potential improvement of the KAGRA sensitivity, based on a model of various realistic sources of losses and their influence on the squeezing amplitude

Titania-doped tantala/silica coatings for gravitational-wave detection

Reducing thermal noise from optical coatings is crucial to reaching the required sensitivity in next generation interferometric gravitational-wave detectors. Here we show that adding TiO2 to Ta2O5 in Ta2O5/SiO2 coatings reduces the internal friction and in addition present data confirming it reduces thermal noise. We also show that TiO2-doped Ta2O5/SiO2 coatings are close to satisfying the optical absorption requirements of second generation gravitational-wave detectors

Immune-Related Gene Expression in Two B-Complex Disparate Genetically Inbred Fayoumi Chicken Lines Following Eimeria maxima Infection

To investigate the influence of genetic differences in the MHC on susceptibility to avian coccidiosis, M5.1 and M15.2 B-haplotype-disparate Fayoumi chickens were orally infected with live Eimeria maxima oocysts, and BW gain, fecal oocyst production, and expression of 14 immune-related genes were determined as parameters of protective immunity. Weight loss was reduced and fecal parasite numbers were lower in birds of the M5.1 line compared with M15.2 line birds. Intestinal intraepithelial lymphocytes from M5.1 chickens expressed greater levels of transcripts encoding interferon-γ (IFN-γ), interleukin-1β (IL-1β), IL-6, IL-8, IL-12, IL-15, IL-17A, inducible nitric oxide synthase, and lipopolysaccharide-induced tumor necrosis factor-α factor and lower levels of mRNA for IFN-α, IL-10, IL-17D, NK-lysin, and tumor necrosis factor superfamily 15 compared with the M15.2 line. In the spleen, E. maxima infection was associated with greater expression levels of IFN-γ, IL-15, and IL-8 and lower levels of IL-6, IL-17D, and IL-12 in M5.1 vs. M15.2 birds. These results suggest that genetic determinants within the chicken MHC influence resistance to E. maxima infection by controlling the local and systemic expression of immune-related cytokine and chemokine genes

The Blue Multi Unit Spectroscopic Explorer (BlueMUSE) on the VLT: characterization of two VPHG prototypes based on dichromated gelatin and photopolymer recording materials

Volume-phase holographic gratings (VPHGs) are widely used in astronomical spectrographs due to their adaptability and high diffraction efficiency. Most VPHGs in operation use dichromated gelatin as a recording material, whose performance is sensitive to the coating and development process, especially in the near-UV. In this letter, we present the characterization of two UV-blue VPHG prototypes for the BlueMUSE integral field spectrograph on the VLT, based on dichromated gelatin and the Bayfol$\circledR$HX photopolymer film as recording materials. Our measurements show that both prototypes meet the required diffraction efficiency and exhibit similar performance with a wavelength-average exceeding 70% in the 350-580 nm range. Deviations from theoretical models increase towards 350 nm, consistently with previous studies on similar gratings. We also report similar performances in terms spatial uniformity and grating-to-grating consistency. Likewise, no significant differences in wavefront error or scattered light are observed between the prototypes.Comment: 7 pages, 5 figures, 1 table. Presented at SPIE "Astronomical Telescopes and Instrumentation", June 2024, in Yokohama, as part of "Advances in Optical and Mechanical Technologies for Telescopes and Instrumentation VI