Gains from the upgrade of the cold neutron triple-axis spectrometer FLEXX at the BER-II reactor

The upgrade of the cold neutron triple-axis spectrometer FLEXX is described. We discuss the characterisation of the gains from the new primary spectrometer, including a larger guide and double focussing monochromator, and present measurements of the energy and momentum resolution and of the neutron flux of the instrument. We found an order of magnitude gain in intensity (at the cost of coarser momentum resolution), and that the incoherent elastic energy widths are measurably narrower than before the upgrade. The much improved count rate should allow the use of smaller single crystals samples and thus enable the upgraded FLEXX spectrometer to continue making leading edge measurements.Comment: 8 pages, 7 figures, 5 table

Critical X-ray Scattering Studies of Jahn-Teller Phase Transitions in TbV1−x_{1-x}Asx_{x}O4_{4}

The critical behaviour associated with cooperative Jahn-Teller phase transitions in TbV$_{1-x}$As$_{x}$O$_{4}$ (where \textit{x} = 0, 0.17, 1) single crystals have been studied using high resolution x-ray scattering. These materials undergo continuous tetragonal $\to$ orthorhombic structural phase transitions driven by Jahn-Teller physics at T$_C$ = 33.26(2) K, 30.32(2) K and 27.30(2) K for \textit{x} = 0, 0.17 and 1 respectively. The orthorhombic strain was measured close to the phase transition and is shown to display mean field behavior in all three samples. Pronounced fluctuation effects are manifest in the longitudinal width of the Bragg scattering, which diverges as a power law, with an exponent given by $x=0.45 \pm 0.04$, on approaching the transition from either above or below. All samples exhibited twinning; however the disordered x = 0.17 sample showed a broad distribution of twins which were stable to relatively low temperatures, well below T$_C$. This indicates that while the orthorhombic strain continues to develop in a conventional mean field manner in the presence of disorder, twin domains are easily pinned by the quenched impurities and their associated random strains.Comment: 8 pages, 6 figure

Critical Phenomena at the Antiferromagnetic Phase Transition of Azurite

We report on high-resolution acoustic, specific-heat and thermal expansion measurements in the vicinity of the antiferromagnetic phase transition at T_N = 1.88 K on a high-quality single crystal of the natural mineral azurite. A detailed investigation of the critical contribution to the various quantities at T_N is presented. The set of critical exponents and amplitude ratios of the singular contributions above and below the transition indicate that the system can be reasonably well described by a three-dimensional Heisenberg antiferromagnet.Comment: 9 pages, 3 figures, proceedings of ICM 2012, JKP

A detailed determination of the a priori mixing angles in non-leptonic decays of hyperons

Non-leptonic Decays of Hyperons can provide a detailed determination of the a priori mixing angles that appear in physical hadrons in the approach in which non-perturbative flavor and parity violations are present in tiny pieces of the hadron mass operator. The determination of such angles in these decays will provide a bench mark to test their necessary universality-like property in other types of decays. Our main result is that the magnitudes of the a priori mixing angles can be determined quite accurately

Azacitidine for treating acute myeloid leukaemia with more than 30% bone marrow blasts: A Single Technology Appraisal

Report commissioned by the NIHR HTA ProgrammeThis report was commissioned by the NIHR HTA Programme as project number 15/64/10

Higher order parametric X-ray spectra in mosaic graphite and single silicon crystals

We have observed up to eight orders (n) in the spectra of parametric x-radiation, in the range 5-40 keV, produced by the interaction of a 90 Mev electron beam with mosaic graphite and 90 and 35 Mev beams with single silicon crystals. The measured yields and intensity ratios, I(2)/I(n= I), in graphite are not in agreement with the theory of PXR for mosaic crystals. In comparison, the yield and ratios of intensities in silicon are close to the predictions of PXR theory for perfect crystals. The bandwidths of spectral lines measured in both silicon and graphite are in good agreement with theoretical predictions, and are determined by the angular field of view of the detector.U.S. Department of EnergyDNANaval Postgraduate SchoolContract No. DE-FG03-91ER8109

Magnetoelastic and structural properties of azurite Cu3(CO3)2(OH)2 from neutron scattering and muon spin rotation

Azurite, Cu3(CO3)2(OH)2, has been considered an ideal example of a one-dimensional (1D) diamond chain antiferromagnet. Early studies of this material imply the presence of an ordered antiferromagnetic phase below $T_N \sim 1.9$ K while magnetization measurements have revealed a 1/3 magnetization plateau. Until now, no corroborating neutron scattering results have been published to confirm the ordered magnetic moment structure. We present recent neutron diffraction results which reveal the presence of commensurate magnetic order in azurite which coexists with significant magnetoelastic strain. The latter of these effects may indicate the presence of spin frustration in zero applied magnetic field. Muon spin rotation, $\mu$SR, reveals an onset of short-range order below 3K and confirms long-range order below $T_N$.Comment: 5 pages, 4 figures, PHYSICAL REVIEW B 81, 140406(R) (2010

Neutron and X-ray Scattering Studies of the Lightly-Doped Spin-Peierls System Cu(1-x)Cd(x)GeO3

Single crystals of the lightly-doped spin-Peierls system Cu(1-x)Cd(x)GeO3 have been studied using bulk susceptibility, x-ray diffraction, and inelastic neutron scattering techniques. We investigate the triplet gap in the magnetic excitation spectrum of this quasi-one dimensional quantum antiferromagnet, and its relation to the spin-Peierls dimerisation order parameter. We employ two different theoretical forms to model the inelastic neutron scattering cross section and chi''(Q,omega), and show the sensitivity of the gap energy to the choice of chi''(Q,omega). We find that a finite gap exists at the spin-Peierls phase transition.Comment: 15 Pages, 7 Figures, Submitted to J. Phys. :Condensed Matte