SYNTHESIS AND ANTIMICROBIAL STUDY OF SOME TRANSITION METAL COMPLEXES OF PICOLINIC ACID HYDRAZIDE

An approach was presented during this text for organizing of has been carried out for the synthesis of (E)-3,4-dichlorobenzylidene picolino hydrazide using 3,4 - trimethoxybenzaldehyde and thio semicarbazide. This work is very effective medicinal hydrazide derivatives are synthesized from Schiff base route. The structure of the ligand TLC and its complexes were carried various spectral studies. The spectrophotometric data just like the transmittance was cogitated within the 350-2500 nm regions and were found. Fourier transform infrared investigation was wont to characterize the grown crystal and assigning the modes of vibrations and to identify the presence of functional groups.&nbsp

SYNTHESIS CHARECTERIZATION OF PYRAZINEAMIDE AND ITS ACETYLCOLINESTERASE INIHIBITION ASSAY

A probe into the literature survey clearly reveals no work has been administered for the synthesis of pyrazinamide(TLC) using Teraphthaldehyde . therefore this study aimed to figure and produce highly effective medicinal hydrazide derivatives are synthesized from Schiff base route. The structure of the ligand THC and its complexes were carried various spectral studies. From these studies, i do know about the knowledge of chemistry and spectroscopy. The main objective of this study is to synthesis of pyrazineamide and teraphthaledehyde to determine the structure through the analytical (elemental and TLC) and spectral (IR, H1 NMR and C13 NMR) methods of characterizatio

HYDROGINATION CATALYST FOR REDUCTION OF BENZALDEHYDE AND ALCOHOL

The superior reduction reaction of amineoffered 68% yield and time stability of successful product benzyl amine yield is 42% with acids or ammonium salt. The pre catalyst(Rh(cod)Cl)2 on reduction realized in bimetallic medium. Rh and Irmetalsthe acid catalyst compressed the reduction of CO group. 95% of selective benzylamine are identified product compared with expected amine (30%)&nbsp

Structural and electrochemical investigation of waste newspaper based electrodes for supercapacitor applications

Abstract There is a general consensus to develop renewable energy storage and conversion technologies to replace fossil fuel energy for sustainable development. Currently, the development of high performance energy storage and conversion devices is an important step on the road to alternative energy technologies. With a special focus on the upgradation of waste to valuable energy, this paper presents an effective synthetic method that utilizes waste newspapers as the precursor to prepare the activated carbon electrodes by the pyrolysis and chemical activation processes. The amorphous nature and surface morphology of the carbon samples were confirmed by XRD and SEM analysis, respectively. Activated waste newspaper carbon (AWNP) showed good electrochemical properties at 800 °C and its specific capacitance at a scan rate of 2 mV/s was found to be 380 F/g. It is important to mention that the source of the raw material is cost effective and suitable for green technology.</jats:p